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Applications Nitrocompounds, Aromatic Nitrophenols, isomeric - Alumina Operating Conditions Sample Dissolved in: iso-octane/ethanol Adsorbent Used: DAI Silica 32-63 Stationary Phase: None Eluent: iso-octane: ethanol: water = 850:1.25:25 Sample Volume: 1 ml Flow rate: 12 ml/min Operating Pressure: 98 psi Column Size: 9mm x 500 mm Temperature: 20ºC Detection: UV detector 251 nm Substances Separated Sample (mg) Retention Volume (ml) 1. benzene 0.5 24 2. o-nitrophenol 0.5 36 3. phenol 0.5 120 4. m-nitrophenol 0.5 180 5. p-nitrophenol 0.5 264 Nitrophenols, isomeric - Silica Operating Conditions Sample Dissolved in: benzene Adsorbent Used: DAI Silica 32-63 Stationary Phase: None Eluent: iso-octane: ethanol: water = 92:7:1 (w/w) Sample Volume: 1 ml Flow rate: 11 ml/min Operating Pressure: 84 psi Column Size: 9mm x 500 mm Temperature: 20ºC Detection: UV detector 251 nm Substances Separated Sample (mg) Retention Volume (ml) 1. o-nitrophenol 0.5 33 2. phenol 0.5 128 3. m-nitrophenol 0.5 198 4. p-nitrophenol 0.5 297 Nitrophenols, isomeric - Silica Operating Conditions Sample Dissolved in: iso-octane/ethanol Adsorbent Used: DAI Silica 32-63 Stationary Phase: None Eluent: iso-octane: ethanol: water = 850:1.25:25 Sample Volume: 1 ml Flow rate: 12 ml/min Operating Pressure: 98 psi Column Size: 9mm x 500 mm Temperature: 20ºC Detection: UV detector 251 nm Substances Separated Sample (mg) Retention Volume (ml) 1. benzene 0.5 24 2. o-nitrophenol 0.5 36 3. phenol 0.5 120 4. m-nitrophenol 0.5 180 5. p-nitrophenol 0.5 264 About Dynamic | Products | Alumina | Why Dynamic | Applications | Technical Info | FAQ/Helpdesk | Catalog | Shop Online News | Blog | Contact Us | Home
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Operating Conditions
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