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Applications

Nitrocompounds, Aromatic

Nitrophenols, isomeric - Alumina

 

Operating Conditions

Sample Dissolved in: iso-octane/ethanol
Adsorbent Used: DAI Silica 32-63
Stationary Phase: None
Eluent: iso-octane: ethanol: water = 850:1.25:25
Sample Volume: 1 ml
Flow rate: 12 ml/min
Operating Pressure: 98 psi
Column Size: 9mm x 500 mm
Temperature: 20ºC
Detection: UV detector 251 nm
Substances Separated Sample (mg) Retention Volume (ml)
1. benzene 0.5 24
2. o-nitrophenol 0.5 36
3. phenol 0.5 120
4. m-nitrophenol 0.5 180
5. p-nitrophenol 0.5 264
Nitrophenols, isomeric - Silica

 

Operating Conditions

Sample Dissolved in: benzene
Adsorbent Used: DAI Silica 32-63
Stationary Phase: None
Eluent: iso-octane: ethanol: water = 92:7:1 (w/w)
Sample Volume: 1 ml
Flow rate: 11 ml/min
Operating Pressure: 84 psi
Column Size: 9mm x 500 mm
Temperature: 20ºC
Detection: UV detector 251 nm
Substances Separated Sample (mg) Retention Volume (ml)
1. o-nitrophenol 0.5 33
2. phenol 0.5 128
3. m-nitrophenol 0.5 198
4. p-nitrophenol 0.5 297
Nitrophenols, isomeric - Silica

 

Operating Conditions

Sample Dissolved in: iso-octane/ethanol
Adsorbent Used: DAI Silica 32-63
Stationary Phase: None
Eluent: iso-octane: ethanol: water = 850:1.25:25
Sample Volume: 1 ml
Flow rate: 12 ml/min
Operating Pressure: 98 psi
Column Size: 9mm x 500 mm
Temperature: 20ºC
Detection: UV detector 251 nm
Substances Separated Sample (mg) Retention Volume (ml)
1. benzene 0.5 24
2. o-nitrophenol 0.5 36
3. phenol 0.5 120
4. m-nitrophenol 0.5 180
5. p-nitrophenol 0.5 264

 

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Dynamic Adsorbents, Inc. 3280 Peachtree Corners Circle, Suite E Norcross, GA 30092  770-817-0123  Toll-Free:  1-866-314-SORB (7672) FAX:  770-455-4380 info@dynamicadsorbents.com