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Applications

Analgesics, Pharmaceutical Formulations

Phenacetin, Acetylsalicylic Acid  - Alumina

 

Operating Conditions

Sample Dissolved in: iso-octane/methylene chloride
Adsorbent Used: DAI Alumina
Stationary Phase: 10% water
Eluent: iso-octane: methylene chloride = 8:2 + 2% acetic acid
Sample Volume: 1 ml
Flow rate: 9 ml/min
Operating Pressure: 30.8 psi
Column Size: 9mm x 300 mm
Temperature: 20ºC
Detection: UV detector 253 nm
Substances Separated Sample (mg) Retention Volume (ml)
1. benzene 1.75 10
2. phenacetin 0.05 67.5
3. acetylsalicylic acid 0.5 130

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Dynamic Adsorbents, Inc. 3280 Peachtree Corners Circle, Suite E Norcross, GA 30092  770-817-0123  Toll-Free:  1-866-314-SORB (7672) FAX:  770-455-4380 info@dynamicadsorbents.com